After trying first few transistors, sample ASIC schematics would be needed to tune the process.
It's important to be sure that these test designs already work in silicon, instead of trying to design or synthesize them from scratch just for testing.
They should be low-tech (not smaller than 0.5um) and should use just 1 or 2 metals.
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Data needed: sample ASIC designs for 1-2 metals
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Re: Data needed: sample ASIC designs for 1-2 metals
Hehe, found nice design 
http://www.4004.com/
All masks are available, 1 metal 1 poly.
It might be tough to do it without poly (i.e. 2 metal no poly).
There is also 6502 ripped pretty well, but it also uses depletion transistors.

http://www.4004.com/
All masks are available, 1 metal 1 poly.
It might be tough to do it without poly (i.e. 2 metal no poly).
There is also 6502 ripped pretty well, but it also uses depletion transistors.
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