Few words about me:From very childhood I loved computers, electronics, lasers, sulfuric acid and liquid nitrogen. I always wanted to be making microchips, UAVs and see nuclear explosion.
Now I am doing software engineering and in the spare time - some microelectronics and physics/chemistry experiments.
I live and work in Russia, Moscow.
Aftermath of X9.3 solar flareSolar minimum they said... It will be spotless they said...
More Deep SpaceFinished processing photos from my last trip so we all can see the results.
Let's start from Milky Way near M6, M7 (exposure 85x3.2s):
Deeper look at the center of our galaxyThis is my first experience in deep sky photography. Best place to start is center of our galaxy - where deep sky objects are densely packed.
128 shots @3.2 seconds exposure each. Sony NEX-5 with Canon FD 55mm F1.email@example.com. All frames were stacked using DeepSkyStacker, plate solving and annotation is done by All Sky Plate Solver. There were 2 shooting sessions for this subject - both at Tenerife mountains, at heights 1500 and 2200 meters. Sky glow was twice brighter at 1500m, so this batch of 106 shots was not used in final stacking. Even at 2200m conditions were far from perfect - wind from Africa carried visible dust which contributed to background brightness.
Next time camera with more modern sensor will help as well as less-bright (!!) lens: F1.2 was making bright stars too large even when stopped down to F2.2. And surely, sky tracking mount will allow much longer exposures and higher image SNR.
On mouse over - annotation. Higher resolution on click.
Chemiluminescence of CPPO with dyes
Finally it worked! It is much more complicated than Luminol reaction. The hardest logistical part was finding CPPO (Bis-[2,4,5-trichloro-6-(pentyloxycarbonyl)phenyl]oxalate). Dyes are Fluorescein and Rhodamine R/6G. Catalyst/acidity regulator is Sodium Acetate (more common bases like NaOH or NaHCO3 were not working). It's conventional synthesis from baking soda and acetic acid is messy and painfully slow - next time going to try synthesis from sodium hydroxide. Sodium acetate is actually a pretty interesting chemical as itself due to interesting phase transitions of it's hydrate - some day I will have some fun with it.
Picking solvent for reaction is another story: components are almost insoluble in water so we have to use some organic solvent. In DMSO (which worked nicely with Luminol) there was some aggressive side reaction. Ethyl acetate has extremely bad smell and is quite unsafe. One of the best and final picks was dibutyl phthalate.
This is not the end of my experiments with CPPO, I still have 99.5g left
Daylight astronomy - VenusIt is believed that city glow at night is a no-go for astronomy. But what about daylight?
I've managed to observe and photograph Venus at noon, when sun was at it's brightest. Without any reference points in the sky and without motorized mount - it's a challenge to spot Venus at daylight. In my binoculars (11x70, with ~4.5° FOV) it was taking couple of minutes using Stellarium and ground reference points.
After that - few more minutes to spot it using main telescope. Venus is no longer a thin sickle - after 3 months Venus and Earth have gone quite far apart on their orbits around the sun:
What's next? Mercury? That's gonna be slightly dangerous... :-)
Sun and AZ5Finally my telescope is on a stable mount - TS AZ5:
Farewell photo of sun spot #2665 in Hβ (486.1nm). Solar minimum is almost there so we are not going to see lots of sunspots during the nearest years.
Fuming nitric acid synthesisIt is not that easy to buy 100% nitric acid due to it's instability (and hence special requirements for transportation) and wide range of it's applications. Distillation does not allow one to get above 68%. If we cannot live without 100% - we'll have to synthesize it ourselves. Last time I did that using quite inconvenient and unsafe method (decomposition of lead(II) nitrate, then dissolving mix of liquid nitrous oxides in 68% nitric acid. This process was too scary to describe in detail
This time I went for conventional and relatively safer route: potassium nitrate (100g) + 98% sulfuric acid (125ml, ~50% excess). You can then distill nearly 100% pure nitric acid.
Final result was reached much easier and faster. Yield was 50ml (which is ~50%, had no more time and ice to continue the process). Next time I will ether have to try something more high-tech (like Peltier cooling with Liebig condenser - Graham's condenser seems to be an overkill and strictly speaking you cannot use it at this angle), or run the process at winter (but it's probably not a good idea to store >100ml of 100% nitric acid due to it's instability).
I've tried a bit of final product right away by etching Texas Instruments IC with very chemically durable plastic.
First light of Skywatcher 120ED refractor telescope - Moon and SaturnJust received my new telescope - Skywatcher 120ED. With my old 10" dobsonian it was almost pointless to observe from the balcony - air turbulence was extremely severe and leaving no chances to catch even single clean frame. That's another reminder than bigger is not always better.
Venus and Saturn today
Good old A77ii+Sony 500F8